HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetic Acid → HCID 836265, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetic Acid | HCID 999 | — |
| Reactant | 2-Amino-4-chlorophenol | HCID 7265 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 836265 | HCID 836265 | — |
Reaction Steps
Phenylacetic acid (20 g, 0.15 mol) in dichloromethane (120 ml) was treated with 1,1′-carbonyl diimidazole (25 g, 0.15 mol). After 1 hour, a solution of 2-hydroxy-5-chloroaniline in dichloromethane was added. The mixture was stirred overnight and processed in the usual manner to give 31.2 g of the title compound as a crystalline solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06372770B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-34fcf0e3520e4cacb32cf5b9d31883ad |
| Source note | uspto-grants-2002_04 |