HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 9901102, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Ethyl 2-benzoyl-4-oxopentanoate | HCID 14689358 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 9901102 | HCID 9901102 | — |
Reaction Steps
Aniline (10 mmol, 0.9 g), 2-benzoyl-4-oxo-pentanoic acid ethyl ester (10 mmol, 2.5 g), and tosic acid (0.1 g) were combined in ethanol, then heated under reflux. The named product was recrystallized from ethanol (m.p. 130° C.-131.7° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06372777B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-c1273095dad94b0591ffdc8b61484f6b |
| Source note | uspto-grants-2002_04 |