HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 10271332, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 3-Bromoaniline | HCID 11562 | — |
| Reactant | Ethyl 2-acetyl-4-oxo-4-phenylbutanoate | HCID 312893 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10271332 | HCID 10271332 | — |
Reaction Steps
m-Bromoaniline (5 mmol, 0.9 g), 3-oxo-2-(2-oxo-2-phenyl-ethyl)-butyric acid ethyl ester (5 mmol, 1.2 g), and tosic acid (0.1 g) were combined in ethanol, then heated under reflux. The named product was recrystallized from ethanol (m.p. 111° C.-112.7° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06372777B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-d45d652959284784b380cfbb656dcb64 |
| Source note | uspto-grants-2002_04 |