HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 10113565, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 3-Iodoaniline | HCID 12271 | — |
| Reactant | Ethyl 2-acetyl-4-oxo-4-phenylbutanoate | HCID 312893 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10113565 | HCID 10113565 | — |
Reaction Steps
m-Iodoaniline (5 mmol, 1.1 g), 3-Oxo-2-(2-oxo-2-phenyl-ethyl)-butyric acid ethyl ester (5 mmol, 1.2 g), and tosic acid (0.1 g) were combined in ethanol, then heated under reflux. The named product was recrystallized in ethanol (m.p. 111° C.-112.9° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06372777B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-24dfe4c3eaf347089c5d1ba597c756ec |
| Source note | uspto-grants-2002_04 |