HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 18373213, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Isatoic Anhydride | HCID 8359 | — |
| Reactant | 6-Aminoindole | HCID 256096 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18373213 | HCID 18373213 | 53% |
Reaction Steps
A mixture of isatoic anhydride (5.06 g, 31 mmol), 6-aminoindole (4.103 g, 31 mmol), toluene (300 mL) and DMF (30 mL) was heated to reflux for 18 hours. The reaction was cooled, filtered, and chromatographed to yield 4.103 g (53%) of the title compound as a tan solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06372759B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-94c70336708844b085e8138569aa44dc |
| Source note | uspto-grants-2002_04 |