HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium;tri(butan-2-yl)boranuide → HCID 11171416, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium;tri(butan-2-yl)boranuide | HCID 4304157 | — |
| Reactant | HCID 11206192 | HCID 11206192 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 11171416 | HCID 11171416 | — |
Reaction Steps
reacting said ethyl (1R,2R)-2-methylcyclohexane-5-one-1-carboxylate (11) with K-Selectride (potassium tri-sec-butylborohydride) in THF at −78° C. to produce ethyl (1R,2R,5S)-5-hydroxy-2-methylcyclohexane-1-carboxylate (12), and
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06375943B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-65eb2bb484354cc0972691ebf2eee7b6 |
| Source note | uspto-grants-2002_04 |