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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 842443Generated: October 31, 2026

Chloride → HCID 11208673, compound

https://huagongshe.com/reaction/842443

Reaction equation

Participants

RoleNameHCIDCharge
ReactantChlorideHCID 312—
ReactantHCID 11171416HCID 11171416—
ReactantHCID 131723184HCID 131723184—
ReactantHCID 131723185HCID 131723185—
SolventCarbon TetrachlorideHCID 5943—
ProductHCID 11208673HCID 11208673—

Reaction Steps

reacting said ethyl (1R,2R,5S)-5-hydroxy-2-methylcyclohexane-1-carboxylate (12) with Ph3P-imidazole-I2 (or Ph3P-2,6-lutidine-I2) in a carbon tetrachloride/methlylene chloride mixture to produce ethyl (1R,2R,5R)-5-iodo-2-methylcyclohexane-1-carboxylate (4a).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06375943B1
Source datasetuspto-grants-2002_04
ORD IDord-9feb0013aa3e4c2c9d55c16ea45d9ecd
Source noteuspto-grants-2002_04