HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Methyl 2-chloro-3-methyl-4-methylsulfonylbenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | 2-Chloro-3-methyl-4-(methylsulfonyl)benzoic acid | HCID 14254476 | — |
| Product | Methyl 2-chloro-3-methyl-4-methylsulfonylbenzoate | HCID 15132838 | — |
Reaction Steps
53.02 g (0.21 mol) of 2-chloro-3-methyl-4-methylsulfonylbenzoic acid were dissolved in 400 ml of methanol and HCl was passed in at reflux temperature for 3 h. The mixture was then allowed to cool and completely concentrated on a rotary evaporator.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06376429B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-745d83b787da4ef9876e46a1ba199dc9 |
| Source note | uspto-grants-2002_04 |