HCID 22614804, compound → HCID 22614814, compound

Participants

Reaction Steps

The product from Example 8D and the product from Example 8E were processed as described in Example 1L to provide the title compound. mp 280-283° C.; [α]23D+19.30° (c 1.03, DMSO); 1H NMR (300 MHz, DMSO-d6) δ2.95-3.80 (m, 7H), 3.80 (s, 3H), 3.86-4.75(m, 6H), 6.44-6.95 (m, 3H), 9.03 (s, 1H), 10.80 (bs, 1H), 13.03 (s, 1H); MS (DCI/NH3) m/e 501 (M+H)+; Anal. calcd for C22H21N6O4SCl.2.2 HCl: C, 45.47; H, 4.02; N, 14.46. Found: C, 45.44; H, 3.81; N, 14.34.

Provenance & Evidence