1-Chloro-4-acetoxynonane → HCID 22615362, compound

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The title compound was prepared from [3-(methanesulfonylamino-methyl)-phenoxy]-acetic acid methyl ester (Preparation 10) and acetic acid 1-(3-chloropropyl)-hexyl ester using the alkylabon procedure described in U.S. Pat. No. 4,033,996. 1H NMR (CDCl3) δ 7.31-7.26 (m, 1H), 7.02-6.84 (m, 3H), 4.68 (s, 2H), 4.35 (s, 2H), 3.91-3.89 (m, 1H), 3.20-3.12 (m, 2H), 2.83 (s, 3H), 1.94-1.92 (m,1H), 1.79-1.24 (m, 12H), 0.87 (t, 3H); MS 400 (M+−1).

Provenance & Evidence