HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 69991071, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 178420709 | HCID 178420709 | — |
| Product | HCID 69991071 | HCID 69991071 | — |
Reaction Steps
To a solution of 0.2 g sodium in 30 ml ethanol is first added 1 g of 5-(4-(3-(2-quinolinylmethyloxy)phenoxymethyl)phenyl)tetrazole and then after 30 minutes 0.6 g of ethylbromoacetate and stirring is continued at 80° C. for 16 hours. The solvent is then removed, diluted with water, filtered, washed with ether and dried to give the desired compound, also referred to as ethyl 5-(4-(3-(2-quinolinylmethyloxy)phenoxymethyl)phenyl)tetrazol-3-yl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06376512B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-68bca9c99f6f4706b8a762da7606cd88 |
| Source note | uspto-grants-2002_04 |