Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 3-Hydroxybenzoic Acid | HCID 7420 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-(Chloromethyl)quinoline hydrochloride | HCID 3083823 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 14774173 | HCID 14774173 | — |
Reaction Steps
A mixture of 28.16 g (0.132 mol) of 2-quinolinylmethyl chloride HCl, 18 g (0.132 mol) of 3-hydroxybenzoic acid and 39.6 g of potassium carbonate in 110 ml of DMF is heated at 70° C. overnight. The reaction mixture is poured into water, and the precipitated product is collected, filtered and dried to give 3-(2quinolinylmethyloxy)benzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06376512B1 |
|---|
| Source dataset | uspto-grants-2002_04 |
|---|
| ORD ID | ord-e0b6207cf6da4e9c94e7259616ad360c |
|---|
| Source note | uspto-grants-2002_04 |
|---|
