Thionyl Chloride → HCID 14774174, compound

HRID 842819Notes

Reaction equation

HRID 842819 reaction equation
[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH2:11][O:12][C:13]1[CH:14]=[C:15]([CH:19]=[CH:20][CH:21]=1)[C:16](O)=[O:17].S(Cl)([Cl:24])=O>>[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH2:11][O:12][C:13]1[CH:14]=[C:15]([CH:19]=[CH:20][CH:21]=1)[C:16]([Cl:24])=[O:17]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 14774173HCID 14774173, compound

Product 1

HCID 14774174HCID 14774174, compound

Procedure

A mixture of 15.6 g (0.1 mol) of 3-(2-quinolinylmethyloxy)benzoic acid and 11.9 g (0.1 mol) of thionyl chloride is refluxed for 4 hours. The reaction mixture is then evaporated to dryness at room temperature and used directly in the next step.

Workup

  1. temperatureis refluxed for 4 hours
  2. customThe reaction mixture is then evaporated to dryness at room temperature

Sources & evidence

ORD record
ord-02c8fd29c27644149bfc81e3ec948c8f
Source dataset
uspto-grants-2002_04
Patent number
US06376512B1

Reaction notes

Loading…