N-bromobutanimide → HCID 15453199, compound

HRID 842878Notes

Reaction equation

[NH2:1][C:2]1[CH:6]=[C:5]([C:7]([CH3:10])([CH3:9])[CH3:8])[O:4][N:3]=1.[Br:11]N1C(=O)CCC1=O>>[NH2:1][C:2]1[C:6]([Br:11])=[C:5]([C:7]([CH3:10])([CH3:9])[CH3:8])[O:4][N:3]=1

Participants

Reactant 2

HCID 67184N-bromobutanimide

HCID 1714733-Isoxazolamine, 5-(1,1-dimethylethyl)-

Product 1

HCID 15453199HCID 15453199, compoundYield 91%

Procedure

This compound was prepared from 3-amino-5-tert-butylisoxazole and N-bromosuccinimide as described in Example 25a in 91% yield, Rf 0.27 (3:1 hexanes/ethyl acetate).

Sources & evidence

ORD record: ord-4b32af8957234db2a6494acefea5ad02
Source dataset: uspto-grants-2002_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06376523B1

Reaction notes

Loading…