Ethyl bromoacetate → HCID 22616832, compound

HRID 843220Notes

Reaction equation

HRID 843220 reaction equation
C([C:3]1[CH:8]=[CH:7][C:6]([N:9]=[N:10][C:11]2[CH:23]=[CH:22][C:14]([O:15][CH2:16][C:17]([O:19][CH2:20][CH3:21])=[O:18])=[CH:13][CH:12]=2)=[CH:5][CH:4]=1)#N.[N+:24](C1C=CC(N=NC2C=CC(O)=CC=2)=CC=1)([O-:26])=[O:25].BrCC(OCC)=O>>[N+:24]([C:3]1[CH:8]=[CH:7][C:6]([N:9]=[N:10][C:11]2[CH:23]=[CH:22][C:14]([O:15][CH2:16][C:17]([O:19][CH2:20][CH3:21])=[O:18])=[CH:13][CH:12]=2)=[CH:5][CH:4]=1)([O-:26])=[O:25]

Participants

4

Reactant 3

HCID 7748Ethyl bromoacetateHCID 150354-[(4-Nitrophenyl)azo]phenolHCID 22616837HCID 22616837, compound

Product 1

HCID 22616832HCID 22616832, compound

Procedure

Ethyl 2-[4-(4-nitrophenylazo)phenoxy]-ethanoate was prepared in a manner similar to ethyl 2-[4-(4-cyanophenylazo)phenoxy]-ethanoate starting from 4-(4-nitrophenylazo)phenol and ethyl bromoacetate.

Sources & evidence

ORD record
ord-9965ca563ea8432cbacd5a23d70223db
Source dataset
uspto-grants-2002_04
Patent number
US06376655B1

Reaction notes

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