HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-[(3-Nitro-4-quinolinyl)amino]ethanol → HCID 13958348, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-[(3-Nitro-4-quinolinyl)amino]ethanol | HCID 13007354 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13958348 | HCID 13958348 | — |
Reaction Steps
2-[(3-Nitro-4-quinolinyl)amino]ethanol (6 g) was combined with ethanol (200 mL) and platinum on carbon catalyst. The mixture was hydrogenated on a Parr apparatus. This procedure was repeated four additional times using a total of 30 g of starting material. The mixtures from all five hydrogenations were combined and then filtered through a layer of Celite® filter aid to remove the catalyst. The filtrate was concentrated under vacuum to provide crude 2-[(3-amino-4-quinolinyl)amino]ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06376669B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-27cd2325c2f04df9afe5d5411b2a525c |
| Source note | uspto-grants-2002_04 |