Trimethylsilyl iodide → HCID 69538513, compound

Participants

Reaction Steps

Compound 11p was synthesized in a similar manner as 11a except that TMS-I was used in place of BBr3. Compound 11p was prepared from compound 12. EI-MS m/z 404 M+; 1H NMR (300 MHz, DMSO-d6) δ 0.98 (s, 3H, CH3), 2.93 (brs, 6H, N(CH3)2), 5.86 (s, 1H, 16-CH), 6.97 (s, 1H, ArH), 7.02 (d, 1H, J=9 Hz, ArH), 7.31 (d, 1H, J=9 Hz, ArH), 7.89 (s, 2H, SO2NH2).

Provenance & Evidence