Dimethylformamide → HCID 22610638, compound

Participants

Reaction Steps

For a period of 0.5 hours, 10 parts of sodium sulfide nonahydrate was added to a solution of 6 parts of 2-(2,7-dinitro-9-fluorenyl)-1,3-dioxolane in 300 parts of dimethylformamide contained within a 1 liter flask at room temperature. The mixture was then stirred for 20 hours, diluted with 1000 parts of methylene chloride, and washed with water in the amount of 4 parts water: 1000 parts methylene chloride.

Provenance & Evidence