HCID 22610640, compound → HCID 22610643, compound

HRID 843495Notes

Reaction equation

HRID 843495 reaction equation
[N+:1]([C:4]1[CH:16]=[CH:15][C:14]2[C:13]3[C:8](=[CH:9][C:10]([N+]([O-])=O)=[CH:11][CH:12]=3)[CH:7]([CH:20]3[O:24][CH2:23][CH2:22][O:21]3)[C:6]=2[CH:5]=1)([O-:3])=[O:2].[O-:25][CH2:26][CH3:27].[K+]>>[CH2:26]([O:25][C:10]1[CH:11]=[CH:12][C:13]2[C:14]3[C:6](=[CH:5][C:4]([N+:1]([O-:3])=[O:2])=[CH:16][CH:15]=3)[CH:7]([CH:20]3[O:21][CH2:22][CH2:23][O:24]3)[C:8]=2[CH:9]=1)[CH3:27]

Participants

3

Reactant 2

HCID 22610640HCID 22610640, compoundHCID 23670592Potassium ethoxide

Product 1

HCID 22610643HCID 22610643, compound

Procedure

Following the same procedure described in Example 1, from 10 parts of 2-(2,7-dinitro-9-fluorenyl)-1,3-dioxolane and 12.5 parts of potassium ethoxide there was obtained 9 parts of product, its 1H and 13C NMR was consistent with the assigned structure.

Workup

  1. customthere was obtained 9 parts of product, its 1H and 13C NMR

Sources & evidence

ORD record
ord-e9609e89a594446bb148e134d8b3b6e6
Source dataset
uspto-grants-2002_04
Patent number
US06379590B1

Reaction notes

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