Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | HCID 22468532 | HCID 22468532 | — |
| Reactant | HCID 178507982 | HCID 178507982 | — |
| Product | HCID 22611715 | HCID 22611715 | — |
Reaction Steps
3.5 ml of isonipecotate is added to a solution of 1.0 g of 4N-benzyl-2-chloro-5-nitropyrimidineamine (Reference Example 2) in 35 ml of acetonitrile and the suspension is stirred overnight. 35 ml of ethanol is added to the suspension, cooled to 5° C. and stirred for 1 hour. Filtration afforded 0.91 g of the yellowish title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06380206B1 |
|---|
| Source dataset | uspto-grants-2002_04 |
|---|
| ORD ID | ord-a309843a164e462884fcff472c3ce782 |
|---|
| Source note | uspto-grants-2002_04 |
|---|
