HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Thiophenecarbonyl chloride → HCID 22611606, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Thiophenecarbonyl chloride | HCID 78928 | — |
| Reactant | 1H-Indol-5-amine, 3-(1,2,3,6-tetrahydro-1-methyl-4-pyridinyl)- | HCID 11148867 | — |
| Product | HCID 22611606 | HCID 22611606 | 33% |
Reaction Steps
Beginning with 1.0 gm (4.4 mMol) 5-amino-3-(1-methyl-1,2,3,6-tetrahydropyridin-4-yl)-1H-indole and 0.494 mL (4.6 mMol) 2-thiophenecarbonyl chloride, 0.489 gm (33.0%) of the title compound were recovered as a bright yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06380201B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-6218291678974ddf8a7a92aa414a6b00 |
| Source note | uspto-grants-2002_04 |