HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzoyl chloride → 6-(2-methylbenzoyl)amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzoyl chloride | HCID 70276 | — |
| Reactant | 6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole | HCID 22611560 | — |
| Product | 6-(2-methylbenzoyl)amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole | HCID 53668579 | 71% |
Reaction Steps
Beginning with 10.4 mg (0.046 mMol) 6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole and 8.9 μL (0.051 mMol) 2-methylbenzoyl chloride, 11.3 mg (71%) of the title compound were recovered as a beige solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06380201B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-0f7b4f2f72c14d9d8dda76da1d23ae47 |
| Source note | uspto-grants-2002_04 |