HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22612863, compound → HCID 9925589, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22612863 | HCID 22612863 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 9925589 | HCID 9925589 | — |
Reaction Steps
A mixture of 2-(4-nitro-1,3-dioxoisoindolin-2-yl)-3-carbamoylpropanoic acid (7.5 mmol) and 10% Pd/C (200 mg) in 20 ml of dimethylformamide is treated with 60 psi of hydrogen in a Parr shaker to afford 2-(4-amino-1,3-dioxoisoindolin-2-yl)-3-carbamoylpropanoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06380239B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-1a6bf916661f493b99fbe25aedc9035a |
| Source note | uspto-grants-2002_04 |