HRID84424

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID67338

1,2-Ethanediamine, N,N,N'-trimethyl-

C5H14N2

结构：O=C(O)c1ccc(N(CCO)C(=O)c2cc3c(s2)-c2ccccc2OCC3)c(Cl)c1

HCID57900330

3-Chloro-4-[[(4,5-dihydrothieno[3,2-d][1]benzoxepin-2-yl)carbonyl](2-hydroxyethyl)amino]benzoic acid

C22H18ClNO5S

PRODUCTS

生成物

结构：CN(C)CCN(C)C(=O)c1ccc(N(CCO)C(=O)c2cc3c(s2)-c2ccccc2OCC3)c(Cl)c1

HCID57900517

未命名化合物

收率 35%

PROCEDURE

实验过程

Following Example 91, 3-chloro-4-(N-(2-hydroxyethyl)-4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxamido)benzoic acid and N1,N1,N2-trimethylethane-1,2-diamine were reacted to give 118 (yield 35% of theoretical). MS: (ESI+) 528.2

WORKUP

后处理

customwere reacted