HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Cyclohexylbutanoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Cyclohexanebutanoic acid | HCID 75200 | — |
| Product | 4-Cyclohexylbutanoyl chloride | HCID 13315625 | — |
Reaction Steps
50 g of 4-cyclohexanebutyric acid are refluxed for 4 hours in 160 ml of thionyl chloride. After evaporation of the excess thionyl chloride, the expected product is distilled off. b.p.=70-80° C. at 400 Pa.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06380230B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-b67d361baaf844d68daab285fd9d6e54 |
| Source note | uspto-grants-2002_04 |