HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2,4-Trimethyl-5-nitrobenzene → 2,4,5-Trimethylaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2,4-Trimethyl-5-nitrobenzene | HCID 69130 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2,4,5-Trimethylaniline | HCID 8717 | 97.2% |
Reaction Steps
19.70 g of 2,4,5-trimethylnitrobenzene are dissolved in 500 ml of ethanol and the solution is then hydrogenated at room temperature and pressure in the presence of 1 g of 5% Pd/C. The catalyst is filtered off on Celite® and the medium is then evaporated to give 15.67 g of the expected compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06380230B1 |
| Source dataset | uspto-grants-2002_04 |
| ORD ID | ord-2587545f4ab348df9337b2853650d7ab |
| Source note | uspto-grants-2002_04 |