HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 844603Generated: October 25, 2026
Dinitrofluorobenzene → N-[3-(perfluorooctyl)phenyl]-2,4-dinitrobenzenamine
https://huagongshe.com/reaction/844603
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dinitrofluorobenzene | HCID 6264 | — |
| Reactant | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Reactant | 3-(Heptadecafluorooctyl)aniline | HCID 4245356 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | N-[3-(perfluorooctyl)phenyl]-2,4-dinitrobenzenamine | HCID 22735001 | 83.2% |
Reaction Steps
A mixture of 3-(perfluoro-n-octyl)benzenamine (2.04 g), 2,4-dinitrofluorobenzene (0.78 g), NMP (8 mL) and triethylamine (0.85 mL) was heated to 70° C. for 16 hr. Extraction and recrystallization from hexane-ethyl acetate gave N-[3-(perfluorooctyl)phenyl]-2,4-dinitrobenzenamine (2.25 g, mp 124.5-125° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06380432B2 |
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| Source dataset | uspto-grants-2002_04 |
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| ORD ID | ord-45b562f6d5b84aa68080dedf0184c3b1 |
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| Source note | uspto-grants-2002_04 |
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