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HRID844850

反应详情

EQUATION

反应方程式

HRID 844850 的结构方程式

REACTANTS

反应物

2
结构：Cc1cccc(Br)c1C(=O)O
HCID2735589

2-Bromo-6-methylbenzoic acid

C8H7BrO2

结构：COC(=O)[C@@H](N)Cc1ccc(-c2c(C)n(C)c(=O)n(C)c2=O)cc1
HCID69336975

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cccc(Br)c1C(=O)N[C@@H](Cc1ccc(-c2c(C)n(C)c(=O)n(C)c2=O)cc1)C(=O)O
HCID69335840

未命名化合物

PROCEDURE

实验过程

N-[(2-bromo-6-methylphenyl)carbonyl]-4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine was prepared from 4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine methyl ester and 2-bromo-6-methylbenzoic acid using the general procedures described in example 7 and was obtained as a white solid: mp 240-242° C. FAB-HRMS m/e calcd for C24H24BrN3O5 (M+H) 514.0978, found 514.0965.

WORKUP

后处理

  1. customwas obtained as a white solid