huagongshe.com
HRID844854

反应详情

EQUATION

反应方程式

HRID 844854 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1c(F)cccc1F
HCID9796

2,6-Difluorobenzoic acid

C7H4F2O2

结构：COC(=O)[C@@H](N)Cc1ccc(-c2c(C)n(C)c(=O)n(C)c2=O)cc1
HCID69336975

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(-c2ccc(C[C@H](NC(=O)c3c(F)cccc3F)C(=O)O)cc2)c(=O)n(C)c(=O)n1C
HCID69337579

未命名化合物

PROCEDURE

实验过程

N-[(2,6-difluorophenyl)carbonyl]-4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine was prepared from 4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine methyl ester and 2,6-difluorobenzoic acid using the general procedures described in example 7 and was obtained as an amorphous white solid. ES-HRMS m/e calcd for C23H21F2N3O5 (M+Na) 480.1483, found 480.1489.

WORKUP

后处理

  1. customwas obtained as an amorphous white solid