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HRID844855

反应详情

EQUATION

反应方程式

HRID 844855 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1c(F)cccc1C(F)(F)F
HCID688123

2-Fluoro-6-(trifluoromethyl)benzoic acid

C8H4F4O2

结构：COC(=O)[C@@H](N)Cc1ccc(-c2c(C)n(C)c(=O)n(C)c2=O)cc1
HCID69336975

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(-c2ccc(C[C@H](NC(=O)c3c(F)cccc3C(F)(F)F)C(=O)O)cc2)c(=O)n(C)c(=O)n1C
HCID69336694

未命名化合物

PROCEDURE

实验过程

N-[(2-fluoro-6-(trifluoromethyl)phenyl)carbonyl]-4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine was prepared from 4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine methyl ester and 2-fluoro-6-(trifluoromethyl)benzoic acid using the general procedures described in example 7 and was obtained as a white solid: mp 218-220° C. ES-HRMS m/e calcd for C25H23F4N3O5 (M+Na) 530.1310, found 530.1317.

WORKUP

后处理

  1. customwas obtained as a white solid