HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methyl-3-oxopentanal → 2-Benzylthio-5-isopropyl-1,2,4-triazolo[1,5-a]pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methyl-3-oxopentanal | HCID 14786268 | — |
| Reactant | HCID 178509291 | HCID 178509291 | — |
| Product | 2-Benzylthio-5-isopropyl-1,2,4-triazolo[1,5-a]pyrimidine | HCID 14155091 | 96% |
Reaction Steps
This material was prepared in 96% yield from 3-amino-5-benzylthio-1,2,4-triazole and 4-methyl-3-oxopentanal following the general procedure described in Example 7. The desired product was isolated as a solid, m.p. 65°-66° C. IR and 1H NMR were in agreement with the assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04755212 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-930bf36b26a74682a9e73b96665457e0 |
| Source note | uspto-grants-1988_07 |