Potassium Carbonate → HCID 86742255, compound

Participants

Reaction Steps

A mixture of 25 g. trans-2-p-hydroxyphenyl-5-pentyl-1,4-dioxane (obtainable by nitration of trans-2-phenyl-5-pentyl-1,4-dioxane, hydrogenation of the trans-2-p-nitrophenyl-5-pentyl-1,4-dioxane obtained to give trans-2-p-aminophenyl-5-pentyl-1,4-dioxane, diazotisation and hydrolysis), 6.9 g. K2CO3, 25 g. K2CO3, 25 g. hexyl iodide and 250 ml. DMF is heated, while stirring, for 16 hours at 80°, then cooled and up as usual. One obtains trans-2-p-hexoxyphenyl-5-pentyl-1,4-dioxane.

Provenance & Evidence