HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → HCID 15594668, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4-Methylphenylglyoxal | HCID 576775 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15594668 | HCID 15594668 | 30% |
Reaction Steps
The procedure of Example 1 was repeated, using 16 g (0.267 mol) of ethylenediamine, 32.0 g (0.216 mol) of 4-methylphenylglyoxal, 450 ml of ethanol and 13.2 g of potassium hydroxide, with the result that 11.0 g of the titled compound was obtained (yield: 30%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04755514 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-fede6181132e42e397af3cc171271e36 |
| Source note | uspto-grants-1988_07 |