Ethylenediamine → HCID 15594672, compound

HRID 845018Notes

Reaction equation

HRID 845018 reaction equation
[CH2:1]([NH2:4])[CH2:2][NH2:3].O.[Cl:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[C:13]([CH:15]=O)=O.[OH-].[K+]>C(O)C>[Cl:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[C:13]1[CH:15]=[N:4][CH:1]=[CH:2][N:3]=1

Participants

5

Reactant 3

HCID 3301EthylenediamineHCID 14797Potassium HydroxideHCID 20133485HCID 20133485, compound

Product 1

HCID 15594672HCID 15594672, compoundYield 492.6%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The procedure of Example 1 was repeated, using 1.96 g (3.16 mmol) of ethylenediamine, 4.9 g (2.13 mmol) of 2-chlorophenylglyoxal monohydrate, 1.6 g of potassium hydroxide and 50 ml of ethanol, with the result that 2.0 g of the titled compound was obtained (yield: 49%).

Sources & evidence

ORD record
ord-6552d80e426242d7bbf0cf4aa6d4e132
Source dataset
uspto-grants-1988_07
Patent number
US04755514

Reaction notes

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