HCID 14853001, compound → Brn 6572492

HRID 845057Notes

Reaction equation

HRID 845057 reaction equation
[C:1]([NH:4][C:5]1[CH:6]=[C:7]2[C:12](=[CH:13][CH:14]=1)[C:11](=O)[CH:10]([CH2:16][C:17]([NH2:19])=[O:18])[CH2:9][CH2:8]2)(=[O:3])[CH3:2].C([NH:23]C1C2C=CC=CC=2C2C(CC(=O)NN=2)C1)(=O)C>>[C:1]([NH:4][C:5]1[CH:14]=[CH:13][C:12]2[C:11]3[CH:10]([CH2:16][C:17](=[O:18])[NH:19][N:23]=3)[CH2:9][CH2:8][C:7]=2[CH:6]=1)(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 14853001HCID 14853001, compoundHCID 20133474HCID 20133474, compound

Product 1

HCID 219045Brn 6572492

Procedure

In a manner similar to that described in Preparation 1(d), 6-acetamido-1-oxo-1,2,3,4-tetrahydro-2-naphthylacetamide (1.55 g) was converted into 6-acetamido4,4a,5,6-tetrahydrobenzo[h]cinnolin-3[2H]-one (0.2 g; mp 259°); ν(Nujol mull) 3330, 3215, 1655, 1610cm-1 ; M+ =257.

Sources & evidence

ORD record
ord-05ed0205dddd4be8be7592c304946341
Source dataset
uspto-grants-1988_07
Patent number
US04755511

Reaction notes

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