Methanol → HCID 20133537, compound

HRID 845080Notes

Reaction equation

HRID 845080 reaction equation
[CH3:1][C:2]([C:5]1[CH:6]=[C:7]([S:16][CH2:17][CH2:18][S:19][CH2:20][CH2:21][CH2:22][C:23]([OH:25])=[O:24])[CH:8]=[C:9]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:10]=1[OH:11])([CH3:4])[CH3:3].S(Cl)(Cl)=O.[CH3:30]O>>[CH3:4][C:2]([C:5]1[CH:6]=[C:7]([S:16][CH2:17][CH2:18][S:19][CH2:20][CH2:21][CH2:22][C:23]([O:25][CH3:30])=[O:24])[CH:8]=[C:9]([C:12]([CH3:13])([CH3:14])[CH3:15])[C:10]=1[OH:11])([CH3:1])[CH3:3]

Participants

4

Reactant 3

HCID 887MethanolHCID 24386Thionyl ChlorideHCID 20133520HCID 20133520, compound

Product 1

HCID 20133537HCID 20133537, compound

Procedure

The title compound was prepared according to the method of Example 8 from the title compound of Example 14 (6.5 g) and thionyl chloride (10 ml) in methyl alcohol (75 ml).

Sources & evidence

ORD record
ord-f21a01eac3bc42318b0640fa35e44214
Source dataset
uspto-grants-1988_07
Patent number
US04755524

Reaction notes

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