HuagongsheHuagongshe Chemistry Print Report · For research reference only
Saccharin → Glycidyl methacrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Saccharin | HCID 5143 | — |
| Reactant | Dimethyl-p-toluidine | HCID 7471 | — |
| Reactant | Dicyandiamide | HCID 10005 | — |
| Reactant | Chlortoluron | HCID 27375 | — |
| Reactant | Tert-butyl cumene peroxide | HCID 76997 | — |
| Reactant | Phosphorohydrazidic acid, diethyl ester | HCID 143340 | — |
| Product | Glycidyl methacrylate | HCID 7837 | — |
Reaction Steps
Mixure A (20.0 g) is mixed with dicyandiamide (0.4 g) and N-(3-chloro-4-methylphenyl)-N',N'-dimethylurea (0.4 g) and the mixture milled in a triple-roll mill until homogeneous. The milled product is then treated with tert.butyl cumyl peroxide (0.5 g), N,N-dimethyl-p-toluidine (0.1 g), o-benzoic sulphimide (0.1 g) and diethyl phosphoro hydrazidate (0.2 g) and mixed until homogeneous.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04755571 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-0e683cd1b9c24f10a8ff55d7aabcd417 |
| Source note | uspto-grants-1988_07 |