Sodium Azide → HCID 13714626, compound

Participants

Reaction Steps

A mixture of 0.125 g of 4-azidoandrost-4-en-3,17-dione in 10 ml of dimethylformamide and 0.4 ml of a 1N sodium azide aqueous solution is stirred and heated at 90°-100° C. for 30 minutes, during which time the evolution of nitrogen is observed. After cooling the reaction mixture is worked up as described in the example 1. There are obtained 0.085 g of the title compound, m.p. 147°-149° C. (dec.).

Provenance & Evidence