Formaldehyde → HCID 20132564, compound

HRID 845282Notes

Reaction equation

HRID 845282 reaction equation
[CH2:1]([N:8]([CH2:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)[OH:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:17]=O.[CH:19]([NH:22][CH:23]([CH3:25])[CH3:24])([CH3:21])[CH3:20]>>[CH2:10]([N:8]([CH2:1][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1)[O:9][CH2:17][N:22]([CH:23]([CH3:25])[CH3:24])[CH:19]([CH3:21])[CH3:20])[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

4

Reactant 3

HCID 712FormaldehydeHCID 7912DiisopropylamineHCID 69297Dibenzylhydroxylamine

Product 1

HCID 20132564HCID 20132564, compound

Procedure

The procedure of Example I is repeated using 21.33 g of dibenzylhydroxylamine, 9.73 g of aqueous formaldehyde (37%) solution and 10.12 g of diisopropylamine, to afford the title compound.

Sources & evidence

ORD record
ord-a05d2013b3244cf5b938c484b175fcad
Source dataset
uspto-grants-1988_07
Patent number
US04757102

Reaction notes

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