HCID 3733625, compound → HCID 11075683, compound

HRID 845322Notes

Reaction equation

HRID 845322 reaction equation
[CH2:1]([N:5]1[C:9](=[O:10])[CH2:8][CH:7]([NH:11][C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[C:6]1=[O:18])[CH2:2][CH2:3][CH3:4].NC1C(=O)N(C2C=CC=CC=2)C(=O)C1>>[CH2:1]([N:5]1[C:9](=[O:10])[CH:8]=[C:7]([NH:11][C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=2)[C:6]1=[O:18])[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 3733625HCID 3733625, compoundHCID 14178390HCID 14178390, compound

Product 1

HCID 11075683HCID 11075683, compoundYield 93%

Procedure

Utilizing the procedure above and substituting N-butylanilinosuccinimide for the 3-amino-N-phenylsuccinimide yields 93% of N-butylanilinomaleimide which upon crystallization from isopropyl alcohol has a m.p. of 128°-130° C. Anal. Calcd. for C14H16N20 2: 68.85; H, 6.56; N, 11.48. Found: C, 68.58; H, 6.45; N, 11.38.

Sources & evidence

ORD record
ord-0b8f18124f844c728108bd5ffa54af96
Source dataset
uspto-grants-1988_07
Patent number
US04757146

Reaction notes

Loading…