HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14003446, compound → HCID 14003453, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14003446 | HCID 14003446 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14003453 | HCID 14003453 | 100.3% |
Reaction Steps
A solution of 8.95 g of the azide from Step C in 75 ml ethanol was hydrogenated over 2 g 10% Pd-C at 45° C. for 5 hr. The solution was then filtered and concentrated to afford 8.3 g 3-amino-1-t-butoxycarbonylmethyl-7-phenylperhydroazepin-2-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04757068 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-b2e88cc1ab134ce6ae5fbeb38e813041 |
| Source note | uspto-grants-1988_07 |