2-(Dimethylamino)ethanol → HCID 54680446, compound

HRID 845424Notes

Reaction equation

HRID 845424 reaction equation
[OH:1][CH:2]1[CH2:6][N:5]([CH2:7][C:8]([NH2:10])=[O:9])[C:4](=[O:11])[CH:3]1[CH:12]1[CH2:16][N:15]([CH2:17][C:18]([NH2:20])=[O:19])[C:14](=[O:21])[CH2:13]1.CN(C)CCO>>[OH:1][C:2]1[CH2:6][N:5]([CH2:7][C:8]([NH2:10])=[O:9])[C:4](=[O:11])[C:3]=1[C:12]1[CH2:16][N:15]([CH2:17][C:18]([NH2:20])=[O:19])[C:14](=[O:21])[CH:13]=1

Participants

3

Reactant 2

HCID 79022-(Dimethylamino)ethanolHCID 70416718HCID 70416718, compound

Product 1

HCID 54680446HCID 54680446, compound

Procedure

In a manner analogous to that described in Example 13, from 1,1',5,5'-tetrahydro-4-hydroxy-2,2'-dioxo-[3,4'-bi-3H-pyrrole]-1,1'-diacetic acid diamide and 5 ml of 2-dimethylaminoethanol there is obtained the N,N-dimethyl-N-ethanolammonium salt of 1,1',5,5'-tetrahydro-4-hydroxy-2,2'-dioxo-[3,4'-bi-2H-pyrrole]-1,1'-diacetic acid diamide in the form of a white powder; melting point 170° (decomposition).

Sources & evidence

ORD record
ord-1e88912733bc48b0ad8fc0884f86b44a
Source dataset
uspto-grants-1988_07
Patent number
US04758575

Reaction notes

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