Dibenzylhydroxylamine → Carbamic acid, N-[3-[[[[[bis(phenylmethyl)amino]oxy]carbonyl]amino]methyl]-3,5,5-trimethylcyclohexyl]-, bis(phenylmethyl)azanyl ester

Participants

Reaction Steps

The procedure of Example 1 is repeated using 10.66 g (50 mmol) of N,N-dibenzylhydroxylamine and 5.56 g (25 mmole) of 3-isocyanatomethyl-3,5,5-trimethylcyclohexylisocyanate. The residue is recrystallized from a 1:1 heptane:toluene solvent mixture to give 11.0 g (68%) of a white soldi, m.p. 139°-146° C.

Provenance & Evidence