HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 845622Generated: October 31, 2026
Benzoyl chloride, 3-chloro- → HCID 14032531, compound
https://huagongshe.com/reaction/845622
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzoyl chloride, 3-chloro- | HCID 69252 | — |
| Reactant | HCID 178480237 | HCID 178480237 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 14032531 | HCID 14032531 | 67.7% |
Reaction Steps
A mixture of 3.0 g of 3-(1-methyl-4-piperidinyl)-1H-indazole and 8 ml of 3-chlorobenzoyl chloride was heated at 100° C. for 2 hours. The reaction was allowed to cool, and ether was added. The resultant solid was collected and recrystallized twice from isopropyl alcohol to yield 3.7 g (67.7%) of product, mp 209°-211° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04758668 |
|---|
| Source dataset | uspto-grants-1988_07 |
|---|
| ORD ID | ord-3a1785863db74389b6ea88577a0e90ff |
|---|
| Source note | uspto-grants-1988_07 |
|---|
