HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 845625Generated: October 30, 2026
4-Chlorobenzoyl chloride → HCID 14032625, compound
https://huagongshe.com/reaction/845625
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | HCID 178462536 | HCID 178462536 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 14032625 | HCID 14032625 | 57% |
Reaction Steps
A mixture of 3.0 g of 3-(1-ethyl-4-piperidinyl)-6-fluoro-1H-indazole and 8 ml of 4-chlorobenzoyl chloride was heated at 100° C. in a steam bath for 4 hrs. Ether was added and the solid was collected. The solid was recrystallized twice from ethanol-ether to yield 2.9 g (57%) of product, mp 240-242° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04758668 |
|---|
| Source dataset | uspto-grants-1988_07 |
|---|
| ORD ID | ord-92f8589ecd3d4673ae92233c87a82cbf |
|---|
| Source note | uspto-grants-1988_07 |
|---|
