HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → Butyl butoxy[(2-methylacryloyl)amino]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Butyl Acetate | HCID 31272 | — |
| Reactant | Acetic acid, hydroxy((1-oxo-2-propenyl)amino)-, butyl ester | HCID 174780 | — |
| Product | Butyl butoxy[(2-methylacryloyl)amino]acetate | HCID 57257779 | — |
Reaction Steps
The reaction product of Example VI was employed. Butanol 130 parts, butyl acetate 130 parts, and concentrated sulfuric acid 3.0 parts were added and the water removed by azeotropic distillation under reduced pressure. An air sparge was used to help prevent premature polymerization. Butanol and butyl acetate were then distilled to yield butyl methacryl amidoglycolate butyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04760168 |
| Source dataset | uspto-grants-1988_07 |
| ORD ID | ord-bb1719937a5d4c6080aa59433d5ab084 |
| Source note | uspto-grants-1988_07 |