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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 845938Generated: October 30, 2026

Dimethyl Sulfate → HCID 20130621, compound

https://huagongshe.com/reaction/845938

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethyl SulfateHCID 6497—
ReactantHCID 20130640HCID 20130640—
SolventDimethylformamideHCID 6228—
ProductHCID 20130621HCID 20130621—

Reaction Steps

using isopropyl 2-chloro-4-fluoro-5-[3,6-dihydro-4-ethyl-5-methyl-2,6-dioxo-1(2H)-pyrimidinyl]-benzoate and dimethyl sulphate in dimethylformamide there is obtained isopropyl 2-chloro-4-fluoro-5-[3,6-dihydro-4-ethyl-3,5-dimethyl-2,6-dioxo-1(2H)-pyrimidinyl]-benzoate, 1H--NMR (CDCl3, 400 MHz) 7.82 ppm (d, 1H), 7.33 ppm (d, 1H), 5.23 ppm (m, 1H), 3.51 ppm (s, 3H), 2.71 ppm (m, 2H), 2.04 ppm (s, 3H), 1.35 ppm (d, 6H), 1.28 ppm (t, 3H),

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04760163
Source datasetuspto-grants-1988_07
ORD IDord-65591aa38427467c9f244574f9a3086f
Source noteuspto-grants-1988_07