HCID 20130623, compound → HCID 67910855, compound

HRID 845962Notes

Reaction equation

HRID 845962 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][C:8]([N:11]2[C:16](=[O:17])[C:15]3[CH2:18][CH2:19][CH2:20][C:14]=3[N:13]([CH3:21])[C:12]2=[O:22])=[CH:7][C:3]=1[C:4]([OH:6])=[O:5]>C(O)(C)(C)C>[Cl:1][C:2]1[CH:10]=[CH:9][C:8]([N:11]2[C:16](=[O:17])[C:15]3[CH2:18][CH2:19][CH2:20][C:14]=3[N:13]([CH3:21])[C:12]2=[O:22])=[CH:7][C:3]=1[C:4]([O:6][C:3]([CH3:7])([CH3:4])[CH3:2])=[O:5]

Participants

3

Reactant 1

HCID 20130623HCID 20130623, compound

Product 1

HCID 67910855HCID 67910855, compound

Reagents, catalysts & solvents 1

HCID 6386tert-ButanolSolvent

Procedure

using 2-chloro-5-(1,2,4,5,6,7-hexahydro-1-methyl-2,4-dioxo-3H-cyclopenta[d]pyrimidin-3-yl)-benzoic acid via the corresponding acid chloride and tert.butanol there is obtained tert.butyl 2-chloro-5-(1,2,4,5,6,7-hexahydro-1-methyl-2,4-dioxo-3H-cyclopenta[d]pyrimidin-3-yl)-benzoate, m.p. 189°-191° C.,

Sources & evidence

ORD record
ord-7ac024fa51c943c9a6edd2076bb3b865
Source dataset
uspto-grants-1988_07
Patent number
US04760163

Reaction notes

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