HRID84599

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID76833

Benzene, 1-chloro-2-isocyanato-

C7H4ClNO

结构：CC(C)(C)OC(=O)N(c1cc2c(cn1)-c1sc(Br)cc1CCO2)C(C)(C)C

HCID57900354

未命名化合物

PRODUCTS

生成物

结构：CC(C)(C)OC(=O)N(c1cc2c(cn1)-c1sc(C(=O)Nc3ccccc3Cl)cc1CCO2)C(C)(C)C

HCID57900446

未命名化合物

收率 61%

PROCEDURE

实验过程

Following Scheme 4, tert-butyl 2-bromo-4,5-dihydropyrido[4,3-b]thieno[2,3-d]oxepin-8-yl(tert-butyl)carbamate and 2-chlorophenylisocyanate were reacted to give tert-Butyl tert-butyl(2-(2-chlorophenylcarbamoyl)-4,5-dihydropyrido[4,3-b]thieno[2,3-d]oxepin-8-yl)carbamate (61%). MS: (ESI+) 528.2

WORKUP

后处理

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