2,2,2-Trifluoroethanesulfonyl chloride → HCID 131717479, compound

HRID 846037Notes

Reaction equation

HRID 846037 reaction equation
[F:1][C:2]([F:9])([F:8])[CH2:3][S:4](Cl)(=[O:6])=[O:5].C(=O)([O-])[O-:11].[Ag+2:14]>>[S:4]([CH2:3][C:2]([F:9])([F:8])[F:1])([O-:11])(=[O:6])=[O:5].[Ag+:14]

Participants

3

Reactant 2

HCID 742422,2,2-Trifluoroethanesulfonyl chlorideHCID 178418647HCID 178418647, compound

Product 1

HCID 131717479HCID 131717479, compoundYield 99%

Procedure

The procedure of Example 2 was used except that the starting material was 4.30 mL of 2,2,2-trifluoroethanesulfonyl chloride. The crude acid was reacted with 10 g of silver carbonate giving after workup 10.63 g (99% yield) of silver tresylate.

Sources & evidence

ORD record
ord-2fb0f7d9db1048188302c269288193b3
Source dataset
uspto-grants-1992_08
Patent number
US05135838

Reaction notes

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